3IL8

CRYSTAL STRUCTURE OF INTERLEUKIN 8: SYMBIOSIS OF NMR AND CRYSTALLOGRAPHY

Experimental procedure

Spacegroup name	P 31 2 1
Unit cell lengths	40.300, 40.300, 90.100
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	? - 2.000
R-factor	0.187
RMSD bond length	0.019
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Number of reflections	5879 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	8.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	20 (mg/ml)
2	1	drop	Tris-HCl	0.1 (M)
3	1	drop	ammonium sulphate	40 (%sat)