3IJ6
CRYSTAL STRUCTURE OF AN UNCHARACTERIZED METAL-DEPENDENT HYDROLASE FROM Lactobacillus acidophilus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2009-07-23 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 170.717, 96.433, 96.033 |
Unit cell angles | 90.00, 90.40, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.22205 |
Rwork | 0.221 |
R-free | 0.26812 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.221 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELX |
Refinement software | REFMAC (5.3.0034) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 1.994 | 1.990 |
Rmerge | 0.900 | |
Number of reflections | 106038 | |
<I/σ(I)> | 5.5 | 0.7 |
Completeness [%] | 99.1 | 93.1 |
Redundancy | 2.1 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 0.1M SODIUM ACETATE, PH 4.5, 25% PEG3350, 10% GLYCEROL, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 294K |