3IHX

Methyltransferase domain of human PR domain-containing protein 10

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Collection date	2009-07-17
Spacegroup name	P 43
Unit cell lengths	94.864, 94.864, 76.769
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	94.860 - 2.500
R-factor	0.24407
Rwork	0.242
R-free	0.29780
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3db5 3ep0
RMSD bond length	0.015
RMSD bond angle	1.742
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.5.0072)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.500
Number of reflections	25428

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5		25% PEG3350, 0.2NH4oAC, Bis -6.5, VAPOR DIFFUSION, HANGING DROP