3IHE
Crystal structure of mouse Bcl-xl mutant (F105A) at pH 6.0
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-08 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 63.151, 63.151, 110.323 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.560 - 3.000 |
R-factor | 0.19455 |
Rwork | 0.192 |
R-free | 0.23947 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pq0 |
RMSD bond length | 0.049 |
RMSD bond angle | 3.728 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.090 | 0.098 |
Number of reflections | 4232 | |
<I/σ(I)> | 16.3 | 3.3 |
Completeness [%] | 91.5 | 50.7 |
Redundancy | 9.4 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 295 | 1.7M Ammonium sulphate, MES, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |