3IHD
Crystal structure of mouse Bcl-xl mutant (Y101A) at pH 5.0
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-08 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.811, 62.811, 111.137 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.240 - 1.880 |
R-factor | 0.17302 |
Rwork | 0.171 |
R-free | 0.21043 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pq0 |
RMSD bond length | 0.023 |
RMSD bond angle | 1.817 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.950 |
High resolution limit [Å] | 1.880 | 1.880 |
Rmerge | 0.080 | 0.080 |
Number of reflections | 16650 | |
<I/σ(I)> | 18.9 | 1.6 |
Completeness [%] | 93.5 | 51.2 |
Redundancy | 10.6 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 295 | 1.4M Ammonium Sulphate, Tri-Na citrate, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |