3IGY
Crystal structures of Leishmania mexicana phosphoglycerate mutase at high cobalt concentrations
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX14.1 |
Synchrotron site | SRS |
Beamline | PX14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.870 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 62.746, 72.111, 129.946 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.011 - 2.003 |
R-factor | 0.1568 |
Rwork | 0.155 |
R-free | 0.19900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.185 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.011 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 40289 | |
Completeness [%] | 99.7 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.3 | 290 | 80mM Ammonium acetate, 40mM trisodium citrate pH 6.0, 24%(w/v) PEG4000, VAPOR DIFFUSION, temperature 290K |