3IG9
Small outer capsid protein (SOC) of bacteriophage RB69
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-BM-C |
| Synchrotron site | APS |
| Beamline | 14-BM-C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-04-15 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.072 |
| Spacegroup name | P 61 |
| Unit cell lengths | 49.128, 49.128, 198.674 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 32.312 - 1.900 |
| R-factor | 0.1837 |
| Rwork | 0.181 |
| R-free | 0.22930 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.764 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 32.000 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.052 |
| Number of reflections | 21202 |
| <I/σ(I)> | 33.2 |
| Completeness [%] | 99.2 |
| Redundancy | 7.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 30% PEG 8000; 0.1 M imidazole; 0.2 M NaCl, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
