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3IF4

Structure from the mobile metagenome of North West Arm Sewage Outfall: Integron Cassette Protein Hfx_Cass5

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2009-02-05
DetectorADSC QUANTUM 315
Wavelength(s)0.9798
Spacegroup nameP 1 21 1
Unit cell lengths61.324, 44.481, 82.462
Unit cell angles90.00, 109.81, 90.00
Refinement procedure
Resolution40.226 - 2.181
R-factor0.1828
Rwork0.178
R-free0.23280
Structure solution methodSAD
RMSD bond length0.005
RMSD bond angle0.876
Data reduction softwareHKL-3000
Data scaling softwareSCALEPACK
Phasing softwarePHENIX
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.240
High resolution limit [Å]2.1802.200
Rmerge0.0930.531
Number of reflections21618
<I/σ(I)>34.62.62
Completeness [%]97.668.6
Redundancy74
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.529429% PEG3350, 0.1 M Hepes pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K

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