3IET
Crystal Structure of 237mAb with antigen
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-002+ |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-05-13 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 277.910, 38.240, 95.910 |
Unit cell angles | 90.00, 108.99, 90.00 |
Refinement procedure
Resolution | 19.860 - 2.200 |
R-factor | 0.2293 |
Rwork | 0.227 |
R-free | 0.27120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1m71 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.187 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX (1.4_4) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.860 | 19.860 | 2.280 |
High resolution limit [Å] | 2.200 | 4.720 | 2.200 |
Rmerge | 0.070 | 0.042 | 0.328 |
Number of reflections | 48616 | ||
<I/σ(I)> | 12.6 | 25.7 | 4.8 |
Completeness [%] | 98.5 | 99.5 | 99.7 |
Redundancy | 7.96 | 8.04 | 8.16 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | PEG MME 5000, ZnCl2, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |