3ID3
Crystal Structure of RseP PDZ2 I304A domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR-H |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-16 |
Detector | BRUKER SMART 6000 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.411, 38.147, 51.265 |
Unit cell angles | 90.00, 102.84, 90.00 |
Refinement procedure
Resolution | 49.983 - 2.010 |
R-factor | 0.1978 |
Rwork | 0.197 |
R-free | 0.22230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zpm |
RMSD bond length | 0.007 |
RMSD bond angle | 0.936 |
Data reduction software | SAINT |
Data scaling software | PROTEUM PLUS (PLUS) |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.983 | 2.110 |
High resolution limit [Å] | 2.010 | 2.010 |
Number of reflections | 10330 | |
<I/σ(I)> | 9.85 | 3.21 |
Completeness [%] | 85.2 | 85.2 |
Redundancy | 1.55 | 0.61 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 4M Sodium Formate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |