3I78
35/99/170/186/220-loops of FXa in SGT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-04-10 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 113.710, 113.710, 52.616 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.940 - 3.000 |
R-factor | 0.211 |
Rwork | 0.208 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3beu |
RMSD bond length | 0.013 |
RMSD bond angle | 1.607 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.000 | 3.050 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.105 | 0.323 |
Number of reflections | 7515 | |
<I/σ(I)> | 11.8 | 2.6 |
Completeness [%] | 97.6 | |
Redundancy | 5.8 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 10.5 | 298 | 2.0 M Ammonium sulfate, 0.1 M CAPS, 75 mM NaCl, 25 mM Benzamidine, pH 10.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |