3I70
Long-wavelength structure of NtA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Detector technology | CCD |
Collection date | 2009-03-15 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.6995 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 80.229, 50.710, 54.187 |
Unit cell angles | 90.00, 117.09, 90.00 |
Refinement procedure
Resolution | 27.960 - 2.300 |
R-factor | 0.221 |
Rwork | 0.221 |
R-free | 0.27600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pxu |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.060 | |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 8736 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | VAPOR DIFFUSION |