3I3Z

Human insulin

Experimental procedure

Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE X11
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	X11
Detector technology	CCD
Detector	MAR CCD 165 mm
Spacegroup name	I 21 3
Unit cell lengths	77.365, 77.365, 77.365
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.235 - 1.600
R-factor	0.1747
Rwork	0.174
R-free	0.19530
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.911
Data reduction software	DENZO
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	54.718
High resolution limit [Å]	1.550
Number of reflections	11350

Crystallization Conditions

crystal ID	method	pH	temperature	details
1