3I2C
Crystal structure of anti-IL-23 antibody CNTO4088
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-03 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | I 4 |
Unit cell lengths | 99.430, 99.430, 115.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.800 |
R-factor | 0.19783 |
Rwork | 0.196 |
R-free | 0.23503 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1eo8 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.310 |
Data reduction software | d*TREK (9.6L) |
Data scaling software | d*TREK (9.6L) |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.169 | 0.549 |
Number of reflections | 13889 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.9 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 3.5 | 293 | 0.1 M CITRATE PH 3.5, 24% PEG 8K, VAPOR DIFFUSION, SITTING DROP, temperature 293K |