3HY5
Crystal structure of CRALBP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-11-06 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97618 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 71.930, 71.930, 303.160 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.130 - 3.040 |
| R-factor | 0.242 |
| Rwork | 0.239 |
| R-free | 0.27200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3hx3 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.741 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.220 |
| High resolution limit [Å] | 3.040 | 3.040 |
| Rmerge | 0.059 | 0.534 |
| Number of reflections | 9692 | 1499 |
| <I/σ(I)> | 22.8 | 4.1 |
| Completeness [%] | 99.5 | 99.6 |
| Redundancy | 10.6 | 9.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 298 | 1M Sodium-potassium tartrate, 0.2M Lithium sulfate, pH 7.0, VAPOR DIFFUSION, temperature 298K |
