3HQM
Structures of SPOP-Substrate Complexes: Insights into Molecular Architectures of BTB-Cul3 Ubiquitin Ligases: SPOPMATHx-CiSBC2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Collection date | 2008-06-12 |
Spacegroup name | P 1 |
Unit cell lengths | 44.281, 48.100, 49.860 |
Unit cell angles | 63.00, 64.04, 62.89 |
Refinement procedure
Resolution | 25.570 - 1.740 |
R-factor | 0.17928 |
Rwork | 0.177 |
R-free | 0.21777 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hqh |
RMSD bond length | 0.009 |
RMSD bond angle | 1.192 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.800 |
High resolution limit [Å] | 1.740 | 1.740 |
Number of reflections | 31963 | |
<I/σ(I)> | 30.3 | 9.5 |
Redundancy | 2 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |