3HQA

Crystal structure of human desarg-C5A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU300
Temperature [K]	298
Detector technology	AREA DETECTOR
Collection date	1991-06-07
Detector	SIEMENS-NICOLET X100
Wavelength(s)	1.5418
Spacegroup name	P 41 21 2
Unit cell lengths	50.610, 50.610, 117.490
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.481 - 2.586
R-factor	0.215
Rwork	0.213
R-free	0.25290
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3CU7 (RESIDUES A681 TO A742)
RMSD bond length	0.009
RMSD bond angle	1.132
Data reduction software	X-GEN
Data scaling software	X-GEN
Phasing software	PHASER
Refinement software	PHENIX (1.5_2)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.500
High resolution limit [Å]	2.580
Number of reflections	5330
Completeness [%]	98.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.8	298	2.4 M sodium chloride, pH 4.8, VAPOR DIFFUSION, HANGING DROP, temperature 298K