3HQ9
CcpA from G. sulfurreducens, S134P variant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X12 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X12 |
| Detector technology | CCD |
| Collection date | 2009-03-28 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.05 |
| Spacegroup name | P 1 |
| Unit cell lengths | 50.899, 55.473, 68.606 |
| Unit cell angles | 104.71, 99.39, 108.97 |
Refinement procedure
| Resolution | 63.920 - 1.520 |
| R-factor | 0.16135 |
| Rwork | 0.160 |
| R-free | 0.18379 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3hq6 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.208 |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 90.000 |
| High resolution limit [Å] | 1.520 |
| Number of reflections | 86506 |
| <I/σ(I)> | 18 |
| Completeness [%] | 90.1 |
| Redundancy | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
