3HQ7
CcpA from G. sulfurreducens, G94K/K97Q/R100I variant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X12 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X12 |
| Detector technology | CCD |
| Collection date | 2007-03-21 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.05 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 99.299, 99.353, 78.225 |
| Unit cell angles | 89.97, 89.98, 90.00 |
Refinement procedure
| Resolution | 70.000 - 2.310 |
| R-factor | 0.2129 |
| Rwork | 0.209 |
| R-free | 0.29373 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3hq6 |
| RMSD bond length | 0.032 |
| RMSD bond angle | 2.783 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 70.000 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 17841 |
| <I/σ(I)> | 15 |
| Completeness [%] | 99.6 |
| Redundancy | 15.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
