3HN8
Crystal structure of synaptotagmin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2000-01-22 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97780 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 205.675, 205.675, 143.125 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.816 - 3.500 |
R-factor | 0.24 |
Rwork | 0.238 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.937 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.630 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.167 | 0.571 |
Number of reflections | 39136 | |
<I/σ(I)> | 10.361 | |
Completeness [%] | 99.7 | 100 |
Redundancy | 5.8 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.4 | 277 | 17% MPD, 50mM CaCl2, 100mM NaCl, pH 5.4, VAPOR DIFFUSION, HANGING DROP, temperature 277K |