3HKE
Tubulin-T138067: RB3 stathmin-like domain complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.978 |
Spacegroup name | P 65 |
Unit cell lengths | 326.710, 326.710, 54.120 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 3.600 |
R-factor | 0.20934 |
Rwork | 0.207 |
R-free | 0.25254 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1sa0 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.626 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.700 |
High resolution limit [Å] | 3.600 | 3.600 |
Number of reflections | 38708 | |
<I/σ(I)> | 14.2 | 2.29 |
Completeness [%] | 98.6 | 88.5 |
Redundancy | 4.88 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | PEG, PIPES BUFFER, pH 7.00, VAPOR DIFFUSION, HANGING DROP, temperature 277K |