Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NW12A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-10-20 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.820, 112.056, 51.881 |
| Unit cell angles | 90.00, 110.75, 90.00 |
Refinement procedure
| Resolution | 43.020 - 1.650 |
| R-factor | 0.16999 |
| Rwork | 0.168 |
| R-free | 0.20180 |
| Structure solution method | MIR |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.571 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.990 | 1.710 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.059 | 0.194 |
| Number of reflections | 61518 | |
| <I/σ(I)> | 15.5 | |
| Completeness [%] | 98.5 | 91.2 |
| Redundancy | 3.7 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 277 | 10% PEG 3000, 1M CHES pH9.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
