3HCL
Helical superstructures in a DNA oligonucleotide crystal
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM16 |
| Synchrotron site | ESRF |
| Beamline | BM16 |
| Detector technology | CCD |
| Collection date | 2007-12-08 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9783 |
| Spacegroup name | P 62 2 2 |
| Unit cell lengths | 38.326, 38.326, 56.821 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 33.190 - 2.590 |
| R-factor | 0.23862 |
| Rwork | 0.237 |
| R-free | 0.27509 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 231d |
| RMSD bond length | 0.013 |
| RMSD bond angle | 2.661 |
| Phasing software | MOLREP (VERSION 10.2.6) |
| Refinement software | REFMAC (5.5.0046) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.000 | 2.630 |
| High resolution limit [Å] | 2.590 | 2.590 |
| Rmerge | 0.046 | |
| Number of reflections | 924 | |
| <I/σ(I)> | 43.8 | 12.5 |
| Completeness [%] | 98.8 | 100 |
| Redundancy | 0.99 | 1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
