3H7G
Apo-FR with AU ions
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL38B1 |
| Synchrotron site | SPring-8 |
| Beamline | BL38B1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-03-08 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1.0395 |
| Spacegroup name | F 4 3 2 |
| Unit cell lengths | 181.632, 181.632, 181.632 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.280 - 1.650 |
| R-factor | 0.21 |
| Rwork | 0.209 |
| R-free | 0.23600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1dat |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.105 |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.000 | 1.710 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.082 | 0.309 |
| Number of reflections | 31508 | |
| <I/σ(I)> | 67.8 | 8.01 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 20.2 | 14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | AMMONIUM SULFATE, CADMIUM SULFATE, VAPOR DIFFUSION, HANGING DROP, temperature 293K | |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | AMMONIUM SULFATE, CADMIUM SULFATE, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
