3H6P
Crystal structure of Rv3019c-Rv3020c from Mycobacterium tuberculosis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-C |
| Synchrotron site | APS |
| Beamline | 24-ID-C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-03-01 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97849 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 40.288, 54.572, 103.101 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 51.570 - 1.910 |
| R-factor | 0.19822 |
| Rwork | 0.196 |
| R-free | 0.23820 |
| Structure solution method | SAD |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.054 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.4.0061) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 80.000 | 1.980 |
| High resolution limit [Å] | 1.910 | 1.910 |
| Number of reflections | 18085 | |
| <I/σ(I)> | 25.5 | 6.1 |
| Completeness [%] | 99.1 | 99.4 |
| Redundancy | 13.7 | 13.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 26% PEG1500, 0.1 M MMT pH 7.0, , VAPOR DIFFUSION, HANGING DROP, temperature 293K |
