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3H47

X-ray Structure of Hexameric HIV-1 CA

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-BM
Synchrotron siteAPS
Beamline22-BM
Collection date2008-07-18
Wavelength(s)1.000
Spacegroup nameP 6
Unit cell lengths90.995, 90.995, 56.853
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution26.740 - 1.900
R-factor0.2342
Rwork0.232
R-free0.26950
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB 2PXR - with residues 1-14 and 87-100 deleted PDB 2BUO - with residues 175-190 deleted
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]1.900
Number of reflections21352
<I/σ(I)>21.1
Completeness [%]99.9
Redundancy10.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.527710-12% PEG 8,000, 100 mM sodium malonate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K

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