3GYE
Didydroorotate dehydrogenase from Leishmania major
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU ULTRAX 18 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 61 |
Unit cell lengths | 143.664, 143.664, 69.750 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.500 - 2.000 |
R-factor | 0.17018 |
Rwork | 0.169 |
R-free | 0.19962 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dor |
RMSD bond length | 0.011 |
RMSD bond angle | 1.202 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 124.035 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.071 |
Number of reflections | 55526 |
<I/σ(I)> | 10.5 |
Completeness [%] | 100.0 |
Redundancy | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | 0.1M Sodium Tribasic Dihydrate pH 5.6, 1M Lithium Sulfate and 0.5M amonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 293K |