3GXM
Crystal structure of acid-beta-glucosidase at pH 4.5, phosphate crystallization condition
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 110.505, 91.779, 152.751 |
Unit cell angles | 90.00, 111.24, 90.00 |
Refinement procedure
Resolution | 34.340 - 2.200 |
R-factor | 0.223 |
Rwork | 0.220 |
R-free | 0.27600 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.682 |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.340 |
High resolution limit [Å] | 2.200 |
Number of reflections | 138784 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | vapor diffusion |