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3GWR

Crystal structure of Putative calcium/calmodulin-dependent protein kinase type II association domain (YP_315894.1) from THIOBACILLUS DENITRIFICANS ATCC 25259 at 2.00 A resolution

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL9-2
Synchrotron siteSSRL
BeamlineBL9-2
Temperature [K]100
Detector technologyCCD
Collection date2009-01-17
DetectorMARMOSAIC 325 mm CCD
Wavelength(s)0.91837,0.97966,0.97951
Spacegroup nameP 21 21 21
Unit cell lengths41.445, 89.655, 90.259
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution28.892 - 2.010
R-factor0.175
Rwork0.173
R-free0.21100
Structure solution methodMAD
RMSD bond length0.016
RMSD bond angle1.588
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareSHELX
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]28.89228.8922.070
High resolution limit [Å]2.0004.3002.000
Rmerge0.0730.0230.586
Number of reflections2272241193711
<I/σ(I)>9.2330.81.4
Completeness [%]94.492.885.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.22770.2000M NH4F, 20.0000% PEG-3350, No Buffer pH 6.2, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K

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