3GTT
Mouse SOD1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-11-18 |
Detector | RIGAKU RAXIS VII |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 112.454, 194.495, 149.841 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.760 - 2.400 |
R-factor | 0.16 |
Rwork | 0.158 |
R-free | 0.19700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vr7 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.076 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 64203 | |
<I/σ(I)> | 11.5 | 2.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 4.2 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 298 | 0.1 M Tris, 30% PEG 1000, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |