3GPG
Crystal structure of macro domain of Chikungunya virus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-06-22 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9330 |
Spacegroup name | P 31 |
Unit cell lengths | 87.061, 87.061, 84.492 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.430 - 1.650 |
R-factor | 0.167 |
Rwork | 0.166 |
R-free | 0.19600 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.337 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 1.740 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.052 | 0.468 |
Number of reflections | 86209 | |
<I/σ(I)> | 3.2 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.7 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 46% PEG 600, 100 mM hepes, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |