3GM7
1.58 A resolution X-ray structure of (CUG)6
Experimental procedure
Spacegroup name | H 3 |
Unit cell lengths | 39.102, 39.102, 141.277 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.600 - 1.580 |
R-factor | 0.227 |
Rwork | 0.219 |
R-free | 0.26200 |
Structure solution method | PDB entry 1ZEV |
RMSD bond length | 0.010 |
RMSD bond angle | 0.028 |
Refinement software | SHELXL-97 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | MOPS, NaCl, MgCl2, MPD, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | MOPS | ||
2 | 1 | 1 | Sodium chloride | ||
3 | 1 | 1 | Magnesium chloride | ||
4 | 1 | 1 | MPD | ||
5 | 1 | 2 | MOPS | ||
6 | 1 | 2 | Sodium chloride | ||
7 | 1 | 2 | Magnesium chloride | ||
8 | 1 | 2 | MPD |