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3GM2

Crystal Structure of the Focal Adhesion Targeting (FAT) Domain of Pyk2

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X29A
Synchrotron siteNSLS
BeamlineX29A
Temperature [K]100
Detector technologyCCD
Collection date2005-02-19
DetectorADSC QUANTUM 315
Wavelength(s)1.1000, 0.9795, 0.9796
Spacegroup nameI 41 2 2
Unit cell lengths82.547, 82.547, 139.528
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.520 - 2.710
R-factor0.261
Rwork0.261
R-free0.29500
Structure solution methodMAD
RMSD bond length0.012
RMSD bond angle1.400
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.800
High resolution limit [Å]2.7002.700
Number of reflections6817
Completeness [%]99.099.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.92983.4 M NaCl, 100 mM HEPES, 1% glycerol, pH 6.9, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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