Loading
PDBj
MenuPDBj@FacebookPDBj@X(formerly Twitter)PDBj@BlueSkyPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3GM2

Crystal Structure of the Focal Adhesion Targeting (FAT) Domain of Pyk2

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X29A
Synchrotron siteNSLS
BeamlineX29A
Temperature [K]100
Detector technologyCCD
Collection date2005-02-19
DetectorADSC QUANTUM 315
Wavelength(s)1.1000, 0.9795, 0.9796
Spacegroup nameI 41 2 2
Unit cell lengths82.547, 82.547, 139.528
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.520 - 2.710
R-factor0.261
Rwork0.261
R-free0.29500
Structure solution methodMAD
RMSD bond length0.012
RMSD bond angle1.400
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.800
High resolution limit [Å]2.7002.700
Number of reflections6817
Completeness [%]99.099.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.92983.4 M NaCl, 100 mM HEPES, 1% glycerol, pH 6.9, VAPOR DIFFUSION, HANGING DROP, temperature 298K

227561

PDB entries from 2024-11-20

PDB statisticsPDBj update infoContact PDBjnumon