3GKH
NPC1(NTD)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Detector technology | CCD |
Collection date | 2008-08-09 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 64 |
Unit cell lengths | 66.181, 66.181, 82.644 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.710 - 1.810 |
R-factor | 0.18189 |
Rwork | 0.180 |
R-free | 0.22082 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.374 |
Refinement software | REFMAC (5.3.0037) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.080 | |
Number of reflections | 18538 | |
Completeness [%] | 98.1 | 98.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 294 | 25% PEG 1500, 100 mM MES Acid, 30 mM Glycine, pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 294K |