3GGH
Donor strand complemented FaeG of F4ad fimbriae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.98340 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 125.029, 125.029, 96.581 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.103 - 1.639 |
R-factor | 0.197 |
Rwork | 0.196 |
R-free | 0.22400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gea |
RMSD bond length | 0.016 |
RMSD bond angle | 1.517 |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.108 | 1.730 |
High resolution limit [Å] | 1.639 | 1.640 |
Rmerge | 0.148 | 0.865 |
Number of reflections | 106726 | |
<I/σ(I)> | 8.4 | 0.5 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 17 | 15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | 20% PEG 4000, 0.2M LiSO4, 0.1M Tris pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |