3G0W
Crystal structure of the rat androgen receptor ligand binding domain complex with an n-aryl-oxazolidin 2-imine inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 32-ID |
| Synchrotron site | APS |
| Beamline | 32-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-12-11 |
| Detector | MAR |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 54.862, 65.739, 69.750 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.840 - 1.950 |
| R-factor | 0.2014 |
| Rwork | 0.200 |
| R-free | 0.23820 |
| Structure solution method | MR |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.806 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | BUSTER-TNT (2.5.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.020 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.085 | 0.452 |
| Number of reflections | 18851 | |
| <I/σ(I)> | 20.6 | 4.6 |
| Completeness [%] | 99.4 | 100 |
| Redundancy | 7.3 | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.88M NA TARTRATE, 0.1M NA HEPES, PH 7.5, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 298K |
