3FVM
Crystal structure of Steptococcus suis mannonate dehydratase with metal Mn++
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-12-10 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 105.690, 105.690, 159.572 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.060 - 2.900 |
R-factor | 0.2368 |
Rwork | 0.234 |
R-free | 0.28585 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1tz9 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.636 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 25673 | |
<I/σ(I)> | 5 | |
Completeness [%] | 94.0 | 95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 0.2M potassium/sodium tartrate, 0.1M sodium citrate, 1M ammonium sulfate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |