3FUY
Structure from the mobile metagenome of Cole Harbour Salt Marsh: Integron Cassette Protein HFX_CASS1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97929 |
Spacegroup name | P 32 |
Unit cell lengths | 71.572, 71.572, 92.725 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.126 - 2.000 |
R-factor | 0.1985 |
Rwork | 0.195 |
R-free | 0.23410 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.989 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 92.850 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.082 | 0.560 |
Total number of observations | 202528 | |
Number of reflections | 35948 | |
<I/σ(I)> | 15.3 | 4.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.6 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 294 | 0.2M ammonium sulfate, 25% PEG 3350 pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 294 | 0.2M ammonium sulfate, 25% PEG 3350 pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |