3FPX
Native fungus laccase from Trametes hirsuta
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-11-11 |
Detector | MAR |
Wavelength(s) | 1.38 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.293, 76.345, 129.661 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.900 - 1.800 |
R-factor | 0.182 |
Rwork | 0.180 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gyc |
RMSD bond length | 0.020 |
RMSD bond angle | 1.826 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.900 | 1.860 |
High resolution limit [Å] | 1.800 | 1.840 |
Rmerge | 0.074 | 0.580 |
Number of reflections | 46382 | |
<I/σ(I)> | 19.8 | 2.7 |
Completeness [%] | 94.7 | 81.3 |
Redundancy | 4.6 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | HANGING DROP | 7 | 299 | 10% PEG 1000, 0.02M potassium phosphate buffer, pH7.0, HANGING DROP, temperature 299.0K |