3FPN
Crystal structure of UvrA-UvrB interaction domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Collection date | 2008-10-08 |
Wavelength(s) | 0.97949 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 84.491, 84.491, 60.874 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.390 - 1.800 |
R-factor | 0.231 |
Rwork | 0.230 |
R-free | 0.24800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2R6F(residues 131-153 and 200-245 chain A) PDB ENTRY 1T5L (residues 157-250 chain A) |
RMSD bond length | 0.012 |
RMSD bond angle | 1.367 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.4.0066) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.830 |
High resolution limit [Å] | 1.800 | 4.880 | 1.800 |
Rmerge | 0.043 | 0.023 | 0.443 |
Number of reflections | 20904 | ||
<I/σ(I)> | 70.679 | ||
Completeness [%] | 99.9 | 98.4 | 100 |
Redundancy | 14.2 | 12.7 | 14.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop vapor diffusion | 5 | 295 | PEG4000, NaCl, sodium acetate, Tris-HCl, pH 5.0, hanging drop vapor diffusion, temperature 295K |