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3FLP

Crystal structure of native heptameric SAP-like pentraxin from Limulus polyphemus

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE PX14.1
Synchrotron siteSRS
BeamlinePX14.1
Temperature [K]100
Detector technologyCCD
Collection date2003-05-06
DetectorADSC
Wavelength(s)1.488
Spacegroup nameP 1 21 1
Unit cell lengths98.320, 167.560, 140.870
Unit cell angles90.00, 92.50, 90.00
Refinement procedure
Resolution45.270 - 2.300
R-factor0.219
Rwork0.201
R-free0.22300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)Dimer created from A subunit of native octameric Limulus SAP
Data reduction softwareMOSFLM
Data scaling softwareSCALA (3.1.4)
Phasing softwareAMoRE
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]45.2702.420
High resolution limit [Å]2.3002.300
Rmerge0.0800.167
Total number of observations54093
Number of reflections180419
<I/σ(I)>5.4353.9
Completeness [%]89.793.2
Redundancy2.12
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.4298PEG 6000, CaCl2, MES, pH 7.4, sitting drop, temperature 298.0K, VAPOR DIFFUSION, SITTING DROP

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