3FK0
E. coli EPSP synthase (TIPS mutation) liganded with S3P
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Collection date | 2008-01-15 |
Detector | RIGAKU RAXIS HTC |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 57.491, 84.705, 87.081 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 20.000 - 1.700 |
Rwork | 0.163 |
R-free | 0.20300 |
Starting model (for MR) | 1g6t |
結合長の平均二乗偏差(RMSD) [Å] | 0.011 |
結合角の平均二乗偏差(RMSD) [度] | 1.600 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | CNS |
Refinement software | CNS |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 20.000 | 1.800 |
分解能 [Å] (高) | 1.700 | 1.700 |
Rmerge_l_obs | 0.029 | 0.077 |
独立反射数 | 47294 | |
<I/σ(I)> | 30.4 | 12.5 |
完全性 [%] | 99.6 | 98.2 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | Na-formate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |