3FJO
Structure of chimeric YH CPR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-31 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 146.800, 60.700, 78.860 |
Unit cell angles | 90.00, 103.36, 90.00 |
Refinement procedure
Resolution | 19.860 - 2.500 |
R-factor | 0.22549 |
Rwork | 0.222 |
R-free | 0.28994 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1AMO (FAD domain) 2BF4 (FMN domain) |
RMSD bond length | 0.008 |
RMSD bond angle | 1.091 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 23129 | |
<I/σ(I)> | 12.7 | 4.2 |
Completeness [%] | 97.4 | 94.9 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | PEGII from Nextal condition G11, pH8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |