3FHU
Crystal structure of type IV b pilin from Salmonella typhi
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12C |
Synchrotron site | NSLS |
Beamline | X12C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-10-09 |
Detector | Brandeis B4 |
Wavelength(s) | 0.97939, 0.97978, 0.95 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 77.880, 114.530, 31.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.100 |
Rwork | 0.220 |
R-free | 0.26000 |
Structure solution method | MAD |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SnB |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 21898 | |
<I/σ(I)> | 26.5 | 7.39 |
Completeness [%] | 95.8 | |
Redundancy | 4.3 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 4M Sodium Formate, VAPOR DIFFUSION, SITTING DROP, temperature 294K |