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3FG8

Crystal structure of PAS domain of RHA05790

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-BM
Synchrotron siteAPS
Beamline19-BM
Temperature [K]100
Detector technologyCCD
Collection date2008-06-27
DetectorCUSTOM-MADE
Wavelength(s)0.97926
Spacegroup nameC 1 2 1
Unit cell lengths149.695, 55.889, 101.856
Unit cell angles90.00, 132.61, 90.00
Refinement procedure
Resolution50.000 - 1.800
R-factor0.17074
Rwork0.168
R-free0.22259
Structure solution methodSAD
RMSD bond length0.014
RMSD bond angle1.547
Data reduction softwareHKL-3000
Data scaling softwareHKL-3000
Phasing softwareHKL-3000
Refinement softwareREFMAC (5.5.0054)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.820
High resolution limit [Å]1.8001.800
Rmerge0.0760.461
Number of reflections57336
<I/σ(I)>30.944.27
Completeness [%]99.499.6
Redundancy7.47.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52970.1M Bis-tris pH6.5, 28%PEG2KMME, VAPOR DIFFUSION, HANGING DROP, temperature 297K

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