3FFM
The crystal structure of human Gadd45g
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Detector technology | CCD |
Collection date | 2007-11-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | I 21 3 |
Unit cell lengths | 126.413, 126.413, 126.413 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.980 - 2.300 |
Rwork | 0.233 |
R-free | 0.25980 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.122 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 13290 |
Redundancy | 10.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 25% PEG 3350, 0.2M Nacl, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |
2 |