3F8M
Crystal Structure of PhnF from Mycobacterium smegmatis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-09-19 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54179 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 64.501, 76.954, 66.897 |
Unit cell angles | 90.00, 113.48, 90.00 |
Refinement procedure
Resolution | 23.240 - 1.800 |
R-factor | 0.215 |
Rwork | 0.213 |
R-free | 0.24800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3f8l |
RMSD bond length | 0.015 |
RMSD bond angle | 1.550 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.3) |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.240 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.085 | 0.466 |
Number of reflections | 55650 | |
<I/σ(I)> | 3.7 | 1.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 4.5 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | 0.1M sodium cacodylate, pH8.0, 0.8M sodium acetate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |