3F7E
MSMEG_3380 F420 Reductase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-04-10 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.863, 65.347, 69.739 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.230 |
R-factor | 0.16816 |
Rwork | 0.167 |
R-free | 0.19104 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.594 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXS |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.000 | 1.300 |
High resolution limit [Å] | 1.230 | 1.230 |
Number of reflections | 73957 | |
<I/σ(I)> | 6.8 | 1.5 |
Completeness [%] | 97.6 | 95.4 |
Redundancy | 6.4 | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291 | 10mM Tris, pH8.5, 20% PEG10000, VAPOR DIFFUSION, HANGING DROP, temperature 291K |