3F6W
XRE-family like protein from Pseudomonas syringae pv. tomato str. DC3000
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-02-03 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97935, 0.97948 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 90.196, 48.306, 111.424 |
| Unit cell angles | 90.00, 98.00, 90.00 |
Refinement procedure
| Resolution | 44.659 - 1.850 |
| R-factor | 0.1934 |
| Rwork | 0.191 |
| R-free | 0.24770 |
| Structure solution method | MAD |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | SHELXD |
| Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.659 | 1.890 |
| High resolution limit [Å] | 1.850 | 1.850 |
| Rmerge | 0.075 | 0.410 |
| Number of reflections | 78813 | |
| <I/σ(I)> | 30.4 | 4 |
| Completeness [%] | 99.2 | 98.4 |
| Redundancy | 7.5 | 7.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 289 | 3M Sodium chloride, 1M Bis-tris, pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 289K |
