3F34
Apoferritin: complex with 2,6-diethylphenol
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X6A |
| Synchrotron site | NSLS |
| Beamline | X6A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-07-05 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9537 |
| Spacegroup name | F 4 3 2 |
| Unit cell lengths | 181.456, 181.456, 181.456 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.670 - 1.680 |
| R-factor | 0.20007 |
| Rwork | 0.198 |
| R-free | 0.24730 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 1xz1 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.392 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | REFMAC (5.4.0074) |
| Refinement software | REFMAC (5.4.0074) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 32.080 | 1.740 |
| High resolution limit [Å] | 1.680 | 1.680 |
| Rmerge | 0.099 | 0.527 |
| Number of reflections | 29091 | |
| <I/σ(I)> | 13 | 2 |
| Completeness [%] | 97.9 | 85.7 |
| Redundancy | 14.83 | 5.26 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | Cadmium sulfate, ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
